Month: December 2012

My first ISIS beamtime

During the last six days, I’ve been in England, more specifically the Rutherford Appleton Laboratory in Oxfordshire, to do measurements on one of our LCO+O crystals (actually the same crystal that we did measurements on at DMC in Switzerland last month). I was at the SXD instrument, a time-of-flight neutron Laue diffractometer, where we measured at five different rotations of the crystal, each for both low temperature and room temperature.

We got a huge amount of data, and mapped out a large volume in reciprocal space. The number of superstructures we saw was really large, and so far we haven’t been able to get a full refinement of the data. The on-site peak integration software was really cool though, and seemed to do the job great – and the instrument scientist was extremely helpful.

All in all, a great experience, and I hope that I (probably with the help of the instrument scientist) will be able to get the superstructures solved.

Of course I also had a few minutes here and there to walk around and take some pictures:

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Posted by PJR in Experiments, Travel, 0 comments